carbon monoxide; palladium on activated charcoal; triphenylphosphine; 1,4-di(diphenylphosphino)-butane in ethylene glycol dimethyl ether
T=100°C; P=30400 Torr; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ali, B. El; Vasapollo, G.; Alper, H.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4739 - 4741
Escourrou
Bulletin de la Societe Chimique de France, 1926 , vol. <4> 39, p. 1465
Bulletin de la Societe Chimique de France, 1928 , vol. <4> 43, p. 1277
in neat (no solvent)
thermolysis on heating to 220°C;;
参考文献
Leonard, N. J.; Sauers, R. R.
Journal of the American Chemical Society, 1957 , vol. 79, p. 6210 - 6214
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Gmelin Handbook: C: MVol.C4, 7.5.5.1.2, page 211 - 212
Berthelot; Gaudechon
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1911 , vol. 152, p. 262
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Berthelot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1914 , vol. 158, p. 1791
in neat (no solvent)
Irradiation (UV/VIS); decomposition by radiation with light below 300 nm at 100-110°C; mechanism discussed;;
参考文献
Berthelot, D.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1914 , vol. 158, p. 1791 - 1793
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Gmelin Handbook: C: MVol.C4, 7.5.5.2, page 212 - 213