反应条件
1: 70 percent / n-BuLi / tetrahydrofuran; hexane / 1.) 0 deg C, 20 min, 2.) 0 deg C, 10 min; room temperature, 30 min
2: 1.) n-BuLi, 2.) CAN, NaHCO3 / 1.) THF, hexane, 0 deg C, 20 min; -30 deg C, 30 min, 2.) CH2Cl2, CH3CN, H2O, -30 deg C, 10 min
3: 60 percent / Bu3SnH, AIBN / benzene / 1 h / 80 °C / Irradiation
View Scheme
参考文献
Chang, Sheng-Yueh; Jiaang, Weir-Torn; Cherng, Chaur-Donp; Tang, Kuo-Hsiang; Huang, Chih-Hao; Tsai, Yeun-Min
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9089 - 9098
