2-氯-1-吗琳乙-1-酮合成路线 (共 27 条)
参考文献
Weissenburger
Patent: DE1000382 , 1955 ;
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Weissenburger
Archiv der Pharmazie (Weinheim, Germany), 1955 , vol. 288, p. 532,535
反应条件
potassium carbonate in tetrahydrofuran T=100°C; 24 h; Heating / reflux;
参考文献
KYOWA HAKKO KOGYO CO., LTD.
Patent: EP1650194 A1, 2006 ;
Location in patent: Page/Page column 34-35 ;
参考文献
Landi-Vittory; Marini-Bettolo
Rend. Ist. super. Sanita, 1956 , vol. 19, p. 109,115
反应条件
in N-methyl-acetamide; methanol; ethanol; acetonitrile
参考文献
Rhone-Poulenc Sante
Patent: US4898871 A1, 1990 ;
参考文献
Wieczorrek; Miliszkiewicz; Lejczak; Soroka; Kafarski
Pesticide Science, 1994 , vol. 40, # 1 p. 57 - 62
反应条件
sodium hydride in tetrahydrofuran
0.2 h; Heating;
参考文献
Schank, Kurt; Bouillon, Guenter; Fuenfrocken, Michael; Lick, Carlo; Lieder, Robert
Helvetica Chimica Acta, 2002 , vol. 85, # 5 p. 1295 - 1326
反应条件
potassium hydroxide in dimethyl sulfoxide
T=35 - 40°C; 1 h;
参考文献
Grasso; Molica; Monforte; Zappala; Trovato
Farmaco, 1995 , vol. 50, # 2 p. 113 - 117
反应条件
sodium azide in N,N-dimethyl-formamide
T=80°C;
参考文献
Swetha; Ramana, P. Venkata; Shirodkar
Organic Preparations and Procedures International, 2011 , vol. 43, # 4 p. 348 - 353
参考文献
Larizza,A.; Brancaccio,G.
Gazzetta Chimica Italiana, 1960 , vol. 90, p. 848 - 862
反应条件
potassium ethyl dithiocarbonate in ethanol
Substitution; 6 h; Heating;
参考文献
Zlatoidsky, Pavol; Maliar, Tibor
European Journal of Medicinal Chemistry, 1999 , vol. 34, # 12 p. 1023 - 1034