3-环戊氧基-4-甲氧基苯甲酸合成路线 （共 7 条）
反应条件
sodium chlorite; aminosulfonic acid; acetic acid 1 h; Ambient temperature;
参考文献
Cook, David C.; Jones, Ronald H.; Kabir, Humayun; Lythgoe, David J.; McFarlane, Ian M.; Pemberton, Clive; Thatcher, Alan A.; Thompson, David M.; Walton, John B.
Organic Process Research and Development, 1998 , vol. 2, # 3 p. 157 - 168
反应条件
sodium chloride in water; acetic acid
参考文献
Cheil Jedang Corp.
Patent: US6103729 A1, 2000 ;
US 6103729 A
反应条件
in water; acetic acid
参考文献
US5935978 A1, ;
US 5935978 A
反应条件
1: 81 percent / K2CO3, KI / dimethylformamide / 21 h / 65 °C 2: 92 percent / sulfamic acid, aq. AcOH, aq. NaClO2 / 1 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 11 p. 1696 - 1703
反应条件
1: 81 percent / K2CO3, KI / dimethylformamide / 21 h / 65 °C 2: 92 percent / sulfamic acid, aq. AcOH, aq. NaClO2 / 1 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 11 p. 1696 - 1703
反应条件
1: 98 percent / SOCl2 / toluene; dimethylformamide / 5 h / Heating 2: Et3N / CH2Cl2 / 5 h / 60 °C View Scheme
参考文献
Ashton, Michael J.; Cook, David C.; Fenton, Garry; Karlsson, Jan-Anders; Palfreyman, Malcolm N.; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 11 p. 1696 - 1703
反应条件
1: 98 percent / SOCl2 / toluene; dimethylformamide / 5 h / Heating 2: 1.) NaH / 1.) THF, 0.25 h, 2.) THF, RT, 0.5 h View Scheme
参考文献
Cook, David C.; Jones, Ronald H.; Kabir, Humayun; Lythgoe, David J.; McFarlane, Ian M.; Pemberton, Clive; Thatcher, Alan A.; Thompson, David M.; Walton, John B.
Organic Process Research and Development, 1998 , vol. 2, # 3 p. 157 - 168
