(4-甲酰苯基)-氨基甲酸叔丁酯合成路线 （共 9 条）
反应条件
manganese(IV) oxide in chloroform T=20°C; 12 h;
参考文献
Schadendorf, Torsten; Hoppmann, Christian; Rueck-Braun, Karola
Tetrahedron Letters, 2007 , vol. 48, # 51 p. 9044 - 9047
反应条件
hydrogenchloride; diisobutylaluminium hydride in methanol; CH2C12; diethyl ether; toluene
参考文献
Ko, Sung-Bo; Oh, Eu-Gene; Kim, Eon-Kyeom; Kim, Won-Yeob; Choi, Dennis W.; Dugan, Laura L.; Koh, Jae-Young; Won, Moo-Ho; Wie, Myung-Bok
Patent: US2003/220337 A1, 2003 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; triethylamine T=90°C; 16 h; Inert atmosphere;
参考文献
Vinogradova, Ekaterina V.; Park, Nathaniel H.; Fors, Brett P.; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 6 p. 1394 - 1397
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); N,N-dicyclohexylmethylamine; potassium formiate; tetra-(n-butyl)ammonium iodide; PCy3∙HBF4; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in acetonitrile T=80°C; 18 h; Sealed tubeGloveboxInert atmosphere;
参考文献
Korsager, Signe; Taaning, Rolf H.; Lindhardt, Anders T.; Skrydstrup, Troels
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 6112 - 6120
反应条件
1: 90 percent / aq. NaOH / dioxane 2: 72 percent / manganese dioxide / CH2Cl2 View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 7 p. 1305 - 1312
反应条件
1: 90 percent / aq. NaOH / dioxane 2: 72 percent / manganese dioxide / CH2Cl2 View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 7 p. 1305 - 1312
反应条件
in dichloromethane; di-tert-butyl dicarbonate
反应条件
1: 83 percent / N,N-diisopropylethylamine / acetonitrile / 96 h / 70 °C 2: 94 percent / diisobutylaluminium hydride / toluene / 2 h / -78 °C 3: 94 percent / MnO2 / CHCl3 / 12 h / 20 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 26 p. 4737 - 4740
反应条件
methanol; tris(acetonitrile)(tricarbonyl)molybdenum T=130°C; 0.25 h; Microwave irradiationInert atmosphere; chemoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3704 - 3710
