1-[2-(甲基硫代)苯基]乙酮合成路线 （共 7 条）
反应条件
1: sodium hydroxide / ethanol / 20 °C 2: iodine / dimethyl sulfoxide / 11 h / 150 °C View Scheme
参考文献
Zheng, Gang; Ma, Xiaoli; Liu, Bangyu; Dong, Ying; Wang, Mang
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 743 - 748
反应条件
sodium methylselenolate in N,N-dimethyl-formamide
8 h; Heating;
参考文献
Evers, Michel; Christiaens, Leon
Tetrahedron Letters, 1983 , vol. 24, # 4 p. 377 - 380
反应条件
1: sodium hydroxide / ethanol / 20 °C
2: iodine / dimethyl sulfoxide / 12 h / 150 °C
View Scheme
参考文献
Zheng, Gang; Ma, Xiaoli; Liu, Bangyu; Dong, Ying; Wang, Mang
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 743 - 748
参考文献
Ruwet,A.; Renson,M.
Bulletin des Societes Chimiques Belges, 1966 , vol. 75, p. 157 - 168
反应条件
1: hydroxylamine hydrochloride / ethanol; pyridine / 4 h / Heating
2: 95 percent / acetic anhydride / pyridine / 24 h / Heating
View Scheme
参考文献
McKinnon, David M.; Lee, Kingsley R.
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1405 - 1409
反应条件
1: 76 percent / 3-chloroperbenzoic acid / CH2Cl2 / 5 - 10 °C
2: 68 percent / LDA / tetrahydrofuran / 10 h / -80 - 20 °C
View Scheme
参考文献
Cabiddu, M.Grazia; Cabiddu, Salvatore; Cadoni, Enzo; Demontis, Stefania; Fattuoni, Claudia; Melis, Stefana
Tetrahedron, 2002 , vol. 58, # 22 p. 4529 - 4533
反应条件
1: 76 percent / 3-chloroperbenzoic acid / CH2Cl2 / 5 - 10 °C
2: 68 percent / LDA / tetrahydrofuran / 10 h / -80 - 20 °C
3: 95 percent / p-toluenesulfonic acid / benzene / Heating
View Scheme
参考文献
Cabiddu, M.Grazia; Cabiddu, Salvatore; Cadoni, Enzo; Demontis, Stefania; Fattuoni, Claudia; Melis, Stefana
Tetrahedron, 2002 , vol. 58, # 22 p. 4529 - 4533
