N,N-二甲基-苯磺酰胺合成路线 （共 44 条）
反应条件
in tetrahydrofuran; water T=0 - 50°C; 1 h;
参考文献
Gavai, Ashvinikumar V.; Norris, Derek J.; Han, Wen-Ching; Vite, Gregory D.; Fink, Brian E.; Tokarski, John S.
Patent: US2005/192310 A1, 2005 ;
Location in patent: Page/Page column 46 ;
参考文献
Silva, A. L.; Covarrubias-Zuniga, A.; Maldonado, L. A.
Organic Preparations and Procedures International, 2002 , vol. 34, # 5 p. 545 - 549
反应条件
sodium hydroxide; potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate in benzene 3.5 h; Heating;
参考文献
Gajda, Tadeusz; Zwierzak, Andrzej
Synthesis, 1981 , # 12 p. 1005 - 1008
反应条件
dimethyl amine in tetrahydrofuran; water
参考文献
Neurosearch A/S.
Patent: US2004/43987 A1, 2004 ;
反应条件
silica column in dichloromethane T=20°C;
参考文献
Banks, Malcolm R.; Hudson, Robert F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 151 - 156
反应条件
1: N-benzenesulfonyl-2,4-dibromopyrrole With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: dimethyl amine in tetrahydrofuran; hexane T=-78 - 0°C; 1.5 h; Inert atmosphere; 3: With methyl chloroformate in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere;
参考文献
Fukuda, Tsutomu; Iwao, Masatomo
Heterocycles, 2012 , vol. 86, # 2 p. 1261 - 1273
反应条件
in dichloromethane T=80°C; 2 h;
参考文献
Knausz, Dezsoe; Meszticzky, Aranka; Szakacs, Laszlo; Csakvari, Bela; Ujszaszy, Kalman
Journal of Organometallic Chemistry, 1983 , vol. 256, # 1 p. 11 - 22
反应条件
diethyl ether T=0°C;
参考文献
Jones; Whalen
Journal of the American Chemical Society, 1925 , vol. 47, p. 1347
反应条件
aluminum oxide; potassium hydroxide T=130°C; 0.0666667 h; microwave irradiation;
参考文献
Malik, Sarika; Nadir, Upender K.; Pandey, Pramod S.
Synthetic Communications, 2008 , vol. 38, # 18 p. 3074 - 3081
反应条件
copper diacetate; 3-phenyl-2-propenoic acid; copper(l) chloride T=110°C; 24 h;
参考文献
Huang, Xin; Wang, Jichao; Ni, Zhangqin; Wang, Sichang; Pan, Yuanjiang
Chemical Communications, 2014 , vol. 50, # 35 p. 4582 - 4584
