N,N-二甲基-苯磺酰胺合成路线 （共 44 条）
反应条件
Cr3(OAc)7(OH)2; periodic acid in acetonitrile T=20°C; 24 h;
参考文献
Xu, Liang; Zhang, Suhong; Trudell, Mark L.
Synlett, 2004 , # 11 p. 1901 - 1904
反应条件
chlorosulfonic acid T=130 - 150°C;
参考文献
Marckwald; v. Droste-Huelshoff
Chem. Zentralbl., 1900 , vol. 71, # I p. 524
Full Text Show Details
Marckwald,W.; v. Droste-Huelshoff
Patent: DE105870 ;
参考文献
Marckwald; v.Droste-Huelshoff
Patent: DE105870 ;
反应条件
water; trifluoroacetic acid T=99°C; determined by 1H NMR; Rate constant;
参考文献
Wagenaar, Anno; Kirby, Anthony J.; Engberts, Jan B. F. N.
Recueil des Travaux Chimiques des Pays-Bas, 1985 , vol. 104, # 7-8 p. 203 - 205
反应条件
1: With n-butyllithium in diethyl ether; hexane T=-78 - 20°C; 1 h; 2: With hydrogenchloride; tri-isopropoxy-borane in diethyl ether; hexane; water T=-78 - 20°C;
参考文献
Gavai, Ashvinikumar V.; Norris, Derek J.; Han, Wen-Ching; Vite, Gregory D.; Fink, Brian E.; Tokarski, John S.
Patent: US2005/192310 A1, 2005 ;
Location in patent: Page/Page column 46 ;
反应条件
dibenzoyl peroxide in tetrachloromethane
Heating;
参考文献
Caristi, Corrado; Ferlazzo, Alida; Gattuso, Mario
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 281 - 285
反应条件
dibenzoyl peroxide in tetrachloromethane
Heating; Yield given;
参考文献
Caristi, C.; Cimino, G.; Ferlazzo, A.; Gattuso, M.; Parisi, M.
Tetrahedron Letters, 1983 , vol. 24, # 26 p. 2685 - 2688
反应条件
n-butyllithium
1.) THF, n-hexane, 0 deg C, 0.5 h 2.) ether; Yield given. Multistep reaction;
参考文献
Wagenaar, Anno; Kirby, Anthony J.; Engberts, Jan B. F. N.
Journal of Organic Chemistry, 1984 , vol. 49, # 19 p. 3445 - 3448
