4-氨基苯基2-乙酰氨基-2-脱氧吡喃己糖苷合成路线 （共 6 条）
反应条件
ammonium formate; palladium on activated charcoal in methanol 0.166667 h; Heating;
参考文献
Roy, Rene; Tropper, Francois D.
Canadian Journal of Chemistry, 1991 , vol. 69, # 5 p. 817 - 821
反应条件
1: 91.3 percent / H2 / 10percent Pd/C / ethanol; dioxane / 3 h / 760 Torr / Ambient temperature 2: 61.8 percent / 28percent NaOMe / methanol; acetonitrile; CHCl3 / 1 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 43, # 2 p. 266 - 270
反应条件
sodium methylate in methanol; chloroform; acetonitrile 1 h; Ambient temperature;
参考文献
Kasai; Okada; Yamaji
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 2 p. 266 - 270
反应条件
1: 46.2 percent / Et3N / acetonitrile / 4 h / 40 °C 2: 91.3 percent / H2 / 10percent Pd/C / ethanol; dioxane / 3 h / 760 Torr / Ambient temperature 3: 61.8 percent / 28percent NaOMe / methanol; acetonitrile; CHCl3 / 1 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 43, # 2 p. 266 - 270
反应条件
1: 73 percent / tetrabutylammonium hydrogen sulfate, 1M NaOH / CH2Cl2 / 0.75 h / Ambient temperature 2: NaOMe / methanol / Ambient temperature 3: 98 percent / ammonium formate / 10percent Pd/C / methanol / 0.17 h / Heating View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 69, # 5 p. 817 - 821
反应条件
1: toluene-4-sulfonic acid 2: palladium/barium sulfate; methanol / Hydrogenation 3: sodium methylate; methanol View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 575, p. 84,89
