anhydrous magnesium perchlorate; 1-(tert-butyldimethylsiloxy)-2-oxa-5-methylbicyclolt;3.1.0gt;hexane; 4-acetyl-benzonitrile; water in acetonitrile
Ambient temperatureIrradiation; Further byproducts given;
参考文献
Abe, Manabu; Oku, Akira
Journal of Organic Chemistry, 1995 , vol. 60, # 10 p. 3065 - 3073
1: in tetrahydrofuran; diethyl ether; tert-butyl methyl ether
T=17 - 23°C; Inert atmosphere;
2: With ammonium chloride in tetrahydrofuran; diethyl ether; tert-butyl methyl ether; water
参考文献
SANOFI-AVENTIS; LEE, George E.; SHRIMP II, Frederick L.; WEIBERTH, Franz J.
Patent: WO2010/107969 A1, 2010 ;
Location in patent: Page/Page column 6-8 ;