3-碘-N-(3,4-二碘苯基)-2-羟基苯甲酰胺合成路线 (共 2 条)
反应条件
triethylamine in tetrahydrofuran T=0 - 25°C; Inert atmosphere;
参考文献
Garner, Amanda L.; Gloeckner, Christian; Tricoche, Nancy; Zakhari, Joseph S.; Samje, Moses; Cho-Ngwa, Fidelis; Lustigman, Sara; Janda, Kim D.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 11 p. 3963 - 3972
反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 25 °C / Inert atmosphere 2: triethylamine / tetrahydrofuran / 0 - 25 °C / Inert atmosphere View Scheme
参考文献
Garner, Amanda L.; Gloeckner, Christian; Tricoche, Nancy; Zakhari, Joseph S.; Samje, Moses; Cho-Ngwa, Fidelis; Lustigman, Sara; Janda, Kim D.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 11 p. 3963 - 3972