3,5-二甲基-2-氨基苯甲酸合成路线 （共 18 条）
反应条件
hydrogenchloride; tin in ethanol; water T=50 - 70°C; 1.5 h;
参考文献
Moorthy, Jarugu Narasimha; Senapati, Kalyan; Parida, Keshaba Nanda; Jhulki, Samik; Sooraj, Kunnikuruvan; Nair, Nisanth N.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9593 - 9601
参考文献
Archiv der Pharmazie (Weinheim, Germany), , p. 583
参考文献
Zhurnal Obshchei Khimii, , vol. 23, p. 606,609; engl. Ausg. S. 629, 632
反应条件
1: 86percent H2SO4 / 1) 55 deg C, 10 min, 2) 75 deg C, 30 min 2: H2O2, NaOH View Scheme
参考文献
Chemische Berichte, , vol. 125, # 4 p. 849 - 856
反应条件
1: fuming nitric acid / Trennung der Saeuren in Form ihrer Bariumsalzes unterhalb 15grad 2: tin; concentrated hydrochloric acid View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 193, p. 162,166
反应条件
1: diluted nitric acid 2: fuming nitric acid / Trennung der Saeuren in Form ihrer Bariumsalzes unterhalb 15grad 3: tin; concentrated hydrochloric acid View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 193, p. 162,166
参考文献
Chemische Berichte, , vol. 34, p. 1323
反应条件
1: With sulfuric acid in water T=25°C; 0.2 h; 2: With sodium nitrite in water T=0°C; 1.5 h; 3: With copper; potassium iodide in water T=25°C; 16 h;
参考文献
Moorthy, Jarugu Narasimha; Senapati, Kalyan; Parida, Keshaba Nanda; Jhulki, Samik; Sooraj, Kunnikuruvan; Nair, Nisanth N.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9593 - 9601
参考文献
Meyer
Monatshefte fuer Chemie, 1904 , vol. 25, p. 1203
反应条件
methyllithium; calcium carbonate
参考文献
Schmitz
Justus Liebigs Annalen der Chemie, 1878 , vol. 193, p. 162,166
