暂无反应条件数据

1: NH3 / methanol / 2 h / Heating 2: 93 percent / Aliquat 336, 50percent aq. NaOH / toluene / 4 h / 20 - 25 °C View Scheme

1: 90 percent / NH3 / methanol / Heating 2: 90 percent / Br2; H2SO4 / acetic acid / 48 h / 20 °C View Scheme

ammonia in methanol Heating;

1: NH3 / methanol / 2 h / Heating 2: 93 percent / Aliquat 336, 50percent aq. NaOH / toluene / 4 h / 20 - 25 °C 3: 81.6 percent / t-BuOK, isoamyl nitrite / toluene / 0.5 h / -20 - 0 °C View Scheme

1: aq. NH3 / ethanol 2: 60 percent / Cs2CO3 / dimethylformamide 3: 1.) KOt-Bu, 2.) 2,4,6-trimethylbenzenesulfonyl azide / 1.) THF, -78 deg C, 2.) THF, -78 deg C 4: PPh3 / tetrahydrofuran; H2O View Scheme

1: NH3 / methanol / 2 h / Heating 2: 93 percent / Aliquat 336, 50percent aq. NaOH / toluene / 4 h / 20 - 25 °C 3: 81.6 percent / t-BuOK, isoamyl nitrite / toluene / 0.5 h / -20 - 0 °C 4: H2 / 5percent Ru/C / methanol / 24 h / 68 - 74 °C / 2068.6 Torr 5: 90 g / 1-hydroxybenzotriazole, 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride, triethylamine / dimethylformamide / 0.25 h / pH = 9.5 6: HCl(g) / ethyl acetate / 0.5 h / 0 °C 7: 1) PhCNS; 2) CF3CO2H / 1) CH2Cl2, reflux, 20 min; 2) 50 deg C, 20 min View Scheme

potassium carbonate in acetonitrile T=60 - 70°C; 2 h;