1.1: hydrogen; 5 palladium on charcoal / acetic acid / 5 h / 7500.75 Torr 2.1: water; acetic acid; sodium nitrite / 20 h / 25 °C 3.1: O-(6-chloro-1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 25 °C / |Inert atmosphere 3.2: 16 h / 25 °C / |Inert atmosphere View Scheme