反应条件
1: 12.3 percent / 1.) α-acetoxyisobutyryl chloride, 2> tri-n-butyltin hydride, 2,2'-azobis<2-methylpropionitrile> / 1.) acetonitrile, 2 h, reflux, 2.) 1,2-dimethoxyethane, 48 h, reflux
2: 22 percent / 1.5 h / Heating
View Scheme
参考文献
Matsuda; Chu; Reichman; et al.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3603 - 3609