N-苯基-氨基磷酸二乙酯合成路线 (共 38 条)
反应条件
sodium hydroxide in toluene 5 h; Reflux;
参考文献
Kaboudin, Babak; Jafari, Ehsan
Synthesis, 2008 , # 17 art. no. Z09508SS, p. 2683 - 2685
反应条件
sodium hydride in N,N-dimethyl-formamide; benzene T=80°C; 5 h;
参考文献
Minami, Toru; Ogata, Masanori; Hirao, Ichiro; Tanaka, Masaya; Agawa, Toshio
Synthesis, 1982 , # 3 p. 231 - 233
反应条件
(i) NaH, dioxane, (ii) CS2, (iii) /BRN= 969135/, benzene; Multistep reaction;
参考文献
Stec,W.J. et al.
Journal of Organic Chemistry, 1976 , vol. 41, # 2 p. 227 - 233
反应条件
in tetrachloromethane T=35°C; other temperature; Product distribution;
参考文献
Challis, Brian C.; Iley, James N.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 1489 - 1494
反应条件
(i) aq. NaOH, <nBu4N>HSO4, (ii) HCl; Multistep reaction;
参考文献
Zwierzak,A.; Brylikowska-Piotrowicz,J.
Angewandte Chemie, 1977 , vol. 89, p. 109 - 110
反应条件
sodium hydride
1) THF, 2) THF.; Yield given. Multistep reaction;
参考文献
Kolodyazhnyi, O. I.; Yakovlev, V. N.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 1 p. 55 - 61,45 - 49
反应条件
in tetrachloromethane
T=80°C; 0.5 h; other time, other molar ratio, study of IR spectra of reaction mixture; Product distribution;
参考文献
Bakhitov, M. I.; Zharkov, V. V.; Kuznetsov, E. V.; Khazeeva, Z. Kh.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 3 p. 552 - 555,432 - 435
反应条件
sodium ethanolate; ethanethiol in ethanol
T=70°C; 2 h;
参考文献
Savignac,P.; Lavielle,G.
Bulletin de la Societe Chimique de France, 1974 , p. 1506 - 1508