in neat (no solvent) in an Schlenk flask (CH3)3Ga was added to freshly sublimed (C6H5)2Hg, the vessel was tightly closed, the suspn. was heated at 100°C for 5h, cooled to room temp.; volatiles were removed under reduced pressure (10 mbar), the residue waswashed twice with n-hexane at -70°C; elem. anal.;
in neat (no solvent) (CH3)3Ga was added to freshly sublimed diphenylmercury, the suspn. was heated at 100°C in a closed vessel for 3 h, cooled to room temp. without stiring; volatiles were removed in vac. (1E-2 mbar), crystals were washed with n-hexane and dried in vac. for 2 h: elem. anal.;
in neat (no solvent) (CH3)3Ga was added to CH3C6H4HgCl, the suspn. was heated at 110°Cfor 5 h in a closed vessel, cooled to room temp.; volatiles were removed under reduced pressure, the residue was washed with n-hexane, dried in vac.; elem. anal.;
Wiberg; Johannsen; Stecher
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1943 , vol. 251, p. 118,123
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Th.Johannsen
Diss.<Muenchen 1941>S.8
