Kraus, C. A.; Toonder, F. E.
Proceedings of the National Academy of Sciences of the United States of America, 1933 , vol. 19, p. 292 - 303
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Gmelin Handbook: Ga: MVol., 39, page 90 - 92
in pentane
under Ar atm. mixt. GaMe3 and GaCl3 in pentane was warmed from -196°C to room temp. and stirred for 12 h; solvent was removed by vac. distillation at room temp., residue was purified by sublimation at room temp.;
参考文献
Beachley Jr.; Rosenblum, Daniel B.; MacRae, David J.
Organometallics, 2001 , vol. 20, # 5 p. 945 - 949
in tetrahydrofuran
Me3Ga adding to a freshly prepared soln. of Na pyrazolate, then tropolone adding to give a yellowish ppt.; refluxing for 40 h, filtering, solidremoving;
参考文献
Rettig; Storr; Trotter
Canadian Journal of Chemistry, 1984 , vol. 62, # 9 p. 1705 - 1708
