(S)-(-)-1-苯基乙醇合成路线 (共 393 条)
反应条件
lipase from Pseudomonas cepacia immobilized on ceramic in toluene T=40°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1151 - 1157
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol T=20°C; 16 h; Title compound not separated from byproducts.;
参考文献
Synthesis, , # 21 p. 3631 - 3638
反应条件
1: With 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane T=20°C; Inert atmosphere; 2: With immobilized Candida antarctica Lipase B; water in hexane T=30°C; pH=6.5; 24 h; aq. phosphate bufferEnzymatic reaction; 3: With water; sodium hydroxide in methanol T=20°C; 1 h; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron, , vol. 66, # 40 p. 8060 - 8067
反应条件
CAL B T=35°C; P=100 Torr; 168 h; Ionic liquidResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 36 p. 6938 - 6943
反应条件
CAL B in acetonitrile T=35°C; 24 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 36 p. 6938 - 6943
反应条件
sodium carbonate; Candida rugosa lipase in toluene T=20°C; 144 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Merabet-Khelassi, Mounia; Houiene, Zahia; Aribi-Zouioueche, Louisa; Riant, Olivier
Tetrahedron Asymmetry, 2012 , vol. 23, # 11-12 p. 828 - 833
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 26, # 1 p. 66 - 71
反应条件
50 U aminoacylase E.C. 3.5.1.14 in hexane T=20°C; Acylation; 168 h;
参考文献
Tetrahedron Asymmetry, , vol. 11, # 8 p. 1801 - 1808
反应条件
50 U aminoacylase E.C. 3.5.1.14 in hexane T=20°C; Acylation; 96 h;
参考文献
Tetrahedron Asymmetry, , vol. 11, # 8 p. 1801 - 1808
反应条件
50 U aminoacylase E.C. 3.5.1.14 in hexane T=20°C; Acylation; 96 h;
参考文献
Tetrahedron Asymmetry, , vol. 11, # 8 p. 1801 - 1808