(S)-(-)-1-苯基乙醇合成路线 （共 393 条）
反应条件
1: 1.) sec-butyllithium / 1.) THF, 2.) ether 2: 91 percent / H2O2, KF, KHCO3 / 15 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 111, # 23 p. 8737 - 8738
反应条件
Candida antarctica lipase B in diethyl ether T=20°C; 144 h; Enzymatic reaction; optical yield given as percent ee;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 10 p. 1191 - 1196
反应条件
CAL B T=35°C; P=100 Torr; 168 h; Ionic liquidResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 36 p. 6938 - 6943
反应条件
CAL B T=35°C; P=100 Torr; 168 h; Ionic liquidResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 36 p. 6938 - 6943
反应条件
water; potassium hydroxide in methanol T=20°C;
参考文献
Journal of the American Chemical Society, , vol. 132, # 47 p. 17041 - 17044
反应条件
toluene-4-sulfonic acid in 1,4-dioxane; tert-butyl methyl ether; water T=40°C; 2 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 9 p. 1737 - 1742
反应条件
2-acetyloxy-1-propene; lipase YS in di-isopropyl ether T=30°C; 19 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 1253 - 1256
反应条件
potassium hydroxide; ethanol; 3-chloro-benzenecarboperoxoic acid 1.) 1,2-dichloroethane, , room temperature, 72 h, 2.) H2O, reflux, 3 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 103, # 11 p. 3088 - 3093
反应条件
in dichloromethane T=0°C; hydroxylation by a chiral iron porphyrin, deuterium isotope effect;
参考文献
Journal of the American Chemical Society, , vol. 111, # 22 p. 8537 - 8538
反应条件
in dichloromethane T=0°C; hydroxylation by a chiral iron porphyrin, deuterium isotope effect;
参考文献
Journal of the American Chemical Society, , vol. 111, # 22 p. 8537 - 8538
