(S)-(-)-1-苯基乙醇合成路线 （共 393 条）
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 20 p. 7092 - 7096
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 20 p. 7092 - 7096
反应条件
sec-alkylsulfatase Pisa1 in dimethyl sulfoxide T=30°C; pH=8.2; 6 h; aq. bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 9 p. 1737 - 1742
反应条件
Candida antarctica lipase B immobilized on supported 1-dodecyl-2-methylimidazolium chloride phase in cyclohexane T=40°C; 3 h; Microwave irradiationResolution of racemateEnzymatic reaction; Reagent/catalyst;
参考文献
RSC Advances, , vol. 3, # 32 p. 13123 - 13126
反应条件
lipase YS in di-isopropyl ether T=30°C; 19 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 1253 - 1256
反应条件
Pseudomonas cepacia lipase in chloroform T=30°C; Esterification; Racemate separation; 55 h; Title compound not separated from byproducts;
参考文献
Synlett, , # 2 p. 225 - 226
反应条件
triphenylphosphine; diethylazodicarboxylate in dichloromethane T=-23 - 20°C; Mitsunobu reaction;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 6 p. 615 - 619
反应条件
aluminium trichloride in hexane; toluene T=-5°C; 17 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 16 p. 1713 - 1719
反应条件
immobilized Candida antarctica Lipase B 18 h;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 13 p. 2130 - 2132
反应条件
1: 41 percent / t-BuOK / tetrahydrofuran / 52 h / Heating 2: KNO2, 18-crown-6 View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 8, # 13 p. 2189 - 2192
