(S)-(-)-1-苯基乙醇合成路线 （共 393 条）
反应条件
sodium hydroxide; Candida rugosa lipase E.(1)C3113 type VII in phosphate buffer T=20°C; pH=7.2; 36 h; Title compound not separated from byproducts.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 24 p. 4439 - 4444
反应条件
lithium hydroxide in methanol 3 h; Heating;
参考文献
Tetrahedron, , vol. 58, # 20 p. 4085 - 4089
反应条件
glutaryl acylase in water T=25°C; pH=7.0; 71 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 14 p. 2509 - 2513
反应条件
glutaryl acylase in methanol; water T=25°C; pH=7.0; 8 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 14 p. 2509 - 2513
反应条件
glutaryl acylase in water T=25°C; pH=7.0; 23 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 14 p. 2509 - 2513
反应条件
1: With D-glucose; β-cyclodextrin in phosphate buffer T=30°C; Baeyer-Villiger oxidation; pH=7.5; 8 h; 2: With Candida antarctica Lipase A in phosphate buffer; hexane 24 h; Further stages. Title compound not separated from byproducts.;
参考文献
Tetrahedron Asymmetry, , vol. 18, # 7 p. 892 - 895
反应条件
1: Candida antarctica B lipase; n-butanol / acetonitrile / 19.2 h 2: aq. LiOH / methanol / 3 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 58, # 20 p. 4085 - 4089
反应条件
1.1: 76 percent / toluene / 4 h / Heating 2.1: n-BuLi; CH2Cl2 / tetrahydrofuran; hexane / -100 °C 2.2: diethyl ether; tetrahydrofuran / -78 - 20 °C 2.3: sodium perborate; aq. NaOH / 16 h View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 657, # 1-2 p. 136 - 145
反应条件
1.1: DMAP / CH2Cl2 / 480 h / 20 °C 1.2: porcine pancreas lipase; poly(ethylene glycol), M.W. ca. 1500 / diisopropyl ether; 1,2-dichloro-benzene / 216 h / 45 °C 2.1: NaOH / tetrahydrofuran / 18 h / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 11, # 6 p. 1279 - 1288
反应条件
1: 48 percent / sodium metaperiodate / methanol / 15 h / Ambient temperature 2: Raney-Ni (W-2), NaPH2O2 / H2O; ethanol / 0.5 h / Ambient temperature; pH=5.2 View Scheme
参考文献
Tetrahedron, , vol. 53, # 38 p. 12883 - 12894
