反应条件
1: 4-(N,N-dimethlyamino)pyridine / diethyl ether / 2 h / 25 °C / |Inert atmosphere 2: sodium tetrahydroborate / ethanol / 2 h / 0 °C / |Inert atmosphere 3: sodium nitrite; acetic acid / dimethyl sulfoxide / 20 h / 40 °C / |Inert atmosphere View Scheme
参考文献
Sleebs, Brad E.; Nguyen, Nghi H.; Hughes, Andrew B.
Synlett, 2013 , vol. 24, # 6 art. no. ST-2012-B0741-L, p. 747 - 751