N-羟基琥珀酰亚胺硬酯酸酯合成路线 (共 9 条)
反应条件
N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide in dichloromethane T=20°C; 21 h;
参考文献
Howarth, Nicola M.; Lindsell, W. Edward; Murray, Euan; Preston, Peter N.
Tetrahedron, 2005 , vol. 61, # 37 p. 8875 - 8887
反应条件
triethylamine in N,N-dimethyl-formamide Inert atmosphereDarkness;
参考文献
Losel, Ralf; Yard, Benito; Beck, Grietje
Patent: US2010/129436 A1, 2010 ;
Location in patent: Page/Page column 4 ;
反应条件
triethylamine in dichloromethane 2.5 h;
参考文献
Eliash, Ran; Weissbuch, Isabelle; Weygand, Markus J.; Kjaer, Kristian; Leiserowitz, Leslie; Lahav, Meir
Journal of Physical Chemistry B, 2004 , vol. 108, # 22 p. 7228 - 7240
反应条件
in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Julina, Radomir; Herzig, Thomas; Bernet, Bruno; Vasella, Andrea
Helvetica Chimica Acta, 1986 , vol. 69, p. 368 - 373
反应条件
hydrogenchloride 1.)dioxane; 100 deg C; 30 min 2.) THF; R.T; 17 h; Multistep reaction;
参考文献
Herold
Helvetica Chimica Acta, 1988 , vol. 71, # 2 p. 354 - 362
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water
T=20°C; 6 h;
参考文献
Yao, Li-Yun; Lin, Qi; Niu, Yin-Yao; Deng, Ke-Min; Zhang, Jian-Hua; Lu, Yang
Molecules, 2009 , vol. 14, # 10 p. 4051 - 4064
反应条件
in tetrahydrofuran
24 h; Ambient temperature;
参考文献
Julina, Radomir; Herzig, Thomas; Bernet, Bruno; Vasella, Andrea
Helvetica Chimica Acta, 1986 , vol. 69, p. 368 - 373
反应条件
hydrogenchloride
1.)dioxane; 100 deg C; 30 min 2.) THF; R.T; 17 h; Multistep reaction;
参考文献
Herold
Helvetica Chimica Acta, 1988 , vol. 71, # 2 p. 354 - 362
反应条件
triethylamine in dichloromethane
2.5 h;
参考文献
Eliash, Ran; Weissbuch, Isabelle; Weygand, Markus J.; Kjaer, Kristian; Leiserowitz, Leslie; Lahav, Meir
Journal of Physical Chemistry B, 2004 , vol. 108, # 22 p. 7228 - 7240