6-甲氧基-1,2,3,4-四氢萘-2-醇合成路线 (共 9 条)
参考文献
A. Christiaens, Societe Anonyme
Patent: US3943172 A1, 1976 ;
反应条件
sodium ethanolate; nickel T=125°C; P=102971 Torr; Hydrogenation;
参考文献
Eriguchi; Takegoshi
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 2 p. 428 - 439
反应条件
trifluoroacetic acid in dichloromethane 2 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Taylor, Stephen K.; Hockerman, Gregory H.; Karrick, Gregory L.; Lyle, Stephen B.; Schramm, Scott B.
Journal of Organic Chemistry, 1983 , vol. 48, # 15 p. 2449 - 2452
反应条件
sodium tetrahydroborate in ethanol T=20°C; 4 h;
参考文献
Tauber, Katharina; Fuchs, Michael; Sattler, Johann H.; Pitzer, Julia; Pressnitz, Desiree; Koszelewski, Dominik; Faber, Kurt; Pfeffer, Jan; Haas, Thomas; Kroutil, Wolfgang
Chemistry - A European Journal, 2013 , vol. 19, # 12 p. 4030 - 4035
参考文献
Clarke; Martini
Journal of the American Chemical Society, 1959 , vol. 81, p. 5716,5721
反应条件
D-glucose in water T=25°C; pH=8; 20 h; aq. potassium phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Zhang, Wei; Tang, Weng Lin; Wang, Zunsheng; Li, Zhi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3380 - 3390
反应条件
H-mordenite in benzene T=80°C; 1 h; var. catalysts, diff. reaction times; Product distribution;
参考文献
Elings, Jacob A.; Downing, Roger S.; Sheldon, Roger A.
European Journal of Organic Chemistry, 1999 , # 4 p. 837 - 846
反应条件
alanine dehydrogenase; (S)-α-alanine; pyridoxal 5'-phosphate; nicotinamide adenine dinucleotide; ammonium chloride; alcohol dehydrogenase in aq. phosphate buffer T=30°C; 24 h; Enzymatic reaction;
参考文献
Tauber, Katharina; Fuchs, Michael; Sattler, Johann H.; Pitzer, Julia; Pressnitz, Desiree; Koszelewski, Dominik; Faber, Kurt; Pfeffer, Jan; Haas, Thomas; Kroutil, Wolfgang
Chemistry - A European Journal, 2013 , vol. 19, # 12 p. 4030 - 4035
反应条件
1: lithium; liquid NH3; diethyl ether / und anschliessend mit Oxalsaeure 2: ethanolic HCl 3: Reduktion mit Lithium in fluessigem NH3 und anschliessendes Hydrolyse mit wss.-methanol.HCl 4: NaBH4 View Scheme
参考文献
Clarke; Martini
Journal of the American Chemical Society, 1959 , vol. 81, p. 5716,5721