sodium methylate in methanol; ethyl acetate

ammonia; water 3 h; Heating;

1: 88 percent / NH3; water / 3 h / Heating 2: 76 percent / DMAP / acetonitrile / 7 h / Heating View Scheme

in methanol; ethyl acetate; methylamine

Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '104767', constants.ctx, '0')">1H-1,2,4-triazol</a> <b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '956581', constants.ctx, '0')">trichlorophosphate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=0 - 20&deg;C;&nbsp;1.16667&nbsp;h;&nbsp;<br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '607626', constants.ctx, '0')">5-methyl-2,4(1H,3H)-pyrimidinedione</a> &nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />9&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br /> <br /> <br /> &nbsp;