反应条件
in acetonitrile N2 atm.; cooling (-78°C), heating (30 min, -40°C), stirring (2 h); extraction (toluene, CH3CN), centrifugation, addn. of toluene, pentane, Et2O, drying (vac., 40°C); elem. anal.;
参考文献
Gereke, Robert; Plinta, Hans-Juergen; Schmutzler, Reinhard
Zeitschrift fur Anorganische und Allgemeine Chemie, 1997 , vol. 623, # 8 p. 1333 - 1343