反应条件
1: 1.) n-BuLi / 1.) THF, 0 deg C, 1 h, 2.) benzene, RT, 2 h
2: 80 percent / Na2CO3, m-chloroperbenzoic acid / CH2Cl2 / 0 °C
3: 5 percent Spectr. / 1.) MgBr2, 2.) n-BuLi / tetrahydrofuran; diethyl ether / 1.) -78 deg C, 10 min, 2a.) -78 deg C, 15 min, 2b.) -78 deg C to 25 deg C, 50 min
View Scheme
参考文献
Jung, Michael E.; Lam, Patrick Yuk-Sun; Mansuri, Muzzamil M.; Speltz, Laurine M.
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1087 - 1105
