[(Pt(.mu.-H)(GeMe3)[P(C6H11)3])2] in hexane
addn. of soln. of Pt-complex to styrene, then addn. of Me3GeH, standing for 48 h; fractional distn.; elem. anal.;
参考文献
Green,M. et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 1519 - 1525
in acetonitrile
byproducts: HNMe2; High Pressure; under inert atm. to soln. Bu3GeNMe2 in MeCN soln. Me3GeH in MeCN was added and heated in tube sealed with Teflon plug at 85°C for 48 h; soln. was allowed to cool, volatiles were removed in vacuo, residue was distilled in Kugelrohr oven (85°C, 0.05 Torr); elem. anal.;
参考文献
Subashi, Esla; Rheingold, Arnold L.; Weinert, Charles S.
Organometallics, 2006 , vol. 25, # 13 p. 3211 - 3219
