反应条件
1: C15H16O With Co(3-Me-5-MeO-salen) in acetonitrile
T=-20 - 20°C; 0.166667 h; Inert atmosphere;
2: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical With dihydrogen peroxide in water; acetonitrile
T=-20°C; 24 h; Inert atmosphere;
3: With hydrogenchloride in water; acetonitrile
T=0 - 20°C; 0.25 h; Inert atmosphere;
参考文献
Watanabe, Eiichi; Kaiho, Atsushi; Kusama, Hiroyuki; Iwasawa, Nobuharu
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11744 - 11747