in ethanol prepn. by mixing hot soln. of metal halide in abs. alc. and phosphane followed by vigorous shaking on electric shaker for about an h; crystals washed (ether); dried over air suction; recrystd.;
参考文献
Evans, R. C.; Mann, F. G.; Peiser, H. S.; Purdie, D.
Journal of the Chemical Society, 1940 , p. 1209 - 1230
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Gmelin Handbook: Hg: MVol.B4, 1.8, page 1339 - 1347
in chloroform refluxing equimolar amts. for 0.5 h, standing overnight; concn., chromy. (SiO2); can be recrystallized (CH2Cl2/petroleum ether); elem. anal.;
参考文献
Liu, Yuan Hong; Wu, Yang Jie; Huo, Shou Quan; Yuan, Han Zhen
Journal of Organometallic Chemistry, 1997 , vol. 534, # 1-2 p. 7 - 13
in chloroform refluxing equimolar amts. for 0.5 h, standing overnight; concn., chromy. (SiO2); can be recrystallized (CH2Cl2/petroleum ether); elem. anal.;
参考文献
Liu, Yuan Hong; Wu, Yang Jie; Huo, Shou Quan; Yuan, Han Zhen
Journal of Organometallic Chemistry, 1997 , vol. 534, # 1-2 p. 7 - 13
in chloroform refluxing equimolar amts. for 0.5 h, standing overnight; concn., chromy. (SiO2); can be recrystallized (CH2Cl2/petroleum ether); elem. anal.;
参考文献
Liu, Yuan Hong; Wu, Yang Jie; Huo, Shou Quan; Yuan, Han Zhen
Journal of Organometallic Chemistry, 1997 , vol. 534, # 1-2 p. 7 - 13
in chloroform refluxing equimolar amts. for 0.5 h, standing overnight; concn., chromy. (SiO2); can be recrystallized (CH2Cl2/petroleum ether); elem. anal.;
参考文献
Liu, Yuan Hong; Wu, Yang Jie; Huo, Shou Quan; Yuan, Han Zhen
Journal of Organometallic Chemistry, 1997 , vol. 534, # 1-2 p. 7 - 13
in chloroform refluxing equimolar amts. for 0.5 h, standing overnight; concn., chromy. (SiO2); can be recrystallized (CH2Cl2/petroleum ether); elem. anal.;
参考文献
Liu, Yuan Hong; Wu, Yang Jie; Huo, Shou Quan; Yuan, Han Zhen
Journal of Organometallic Chemistry, 1997 , vol. 534, # 1-2 p. 7 - 13
triphenyl phosphine in tetrahydrofuran addn. of a THF soln. of PPh3 to a suspn. of the complex in THF, refluxed for 20 min; reduced in vol., cooled, filtered, washed with ether;
参考文献
Pettinari, C.; Santini, C.; Leonesi, D.; Cecchi, P.
Polyhedron, 1994 , vol. 13, p. 1553 - 1562
