反应条件
1: 1.) MsCl, pyridine, 2.) NBu4I, BaCO3, pyridine 2: Hg(OAc)2 3: 1.) BSA, 2.) TMSTf / 1.) MeCN, reflux, 2.) room temperature, 7 h 4: 69 percent / BBr3 / CH2Cl2 / 0.25 h / -78 °C View Scheme
参考文献
Leydier; Bellon; Barascut; Deydier; Maury; Pelicano; Abdelaziz El Alaoui; Imbach
Nucleosides and Nucleotides, 1994 , vol. 13, # 10 p. 2035 - 2050