2,7-二碘-9,9-二甲基芴合成路线 (共 1 条)
反应条件
1: 2,7-diiodofluorene With potassium tert-butylate in tetrahydrofuran; tert-butyl alcohol T=0°C; Inert atmosphere; 2: methyl iodide in tetrahydrofuran; tert-butyl alcohol T=25°C; 1 h; Inert atmosphere; 3: methyl iodide With potassium tert-butylate in tetrahydrofuran; tert-butyl alcohol T=0 - 25°C; Inert atmosphere;
参考文献
West, Kara; Wang, Changsheng; Batsanov, Andrei S.; Bryce, Martin R.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 11 p. 1934 - 1937