1,1,1-三甲基-2,2,2-三苯基二硅烷合成路线 （共 48 条）
反应条件
bis-trimethylsilyl ether; CDD; dimethyl sulfoxide
Irradiation;
参考文献
Swaim,R.E.; Weber,W.P.
Journal of the American Chemical Society, 1979 , vol. 101, p. 5703 - 5706
反应条件
CDD; dimethyl sulfoxide in tetrahydrofuran
Irradiation;
参考文献
Swaim,R.E.; Weber,W.P.
Journal of the American Chemical Society, 1979 , vol. 101, p. 5703 - 5706
反应条件
potassium-sodium in diethyl ether
treatment of (C6H5)3SiSi(CH3)3 in abs. ether at room temp. with a suspn. of liq. Na/K alloy (1:5) in ether;;
参考文献
Gilman; Wu
Journal of the American Chemical Society, 1951 , vol. 73, p. 4031
Journal of Organic Chemistry, 1953 , vol. 18, p. 753,755
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Gilman, H.; Wu, T. C.
Journal of Organic Chemistry, 1953 , vol. 18, p. 753 - 764
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Gmelin Handbook: Si: MVol.C, 116, page 326 - 328
反应条件
hydrogenchloride; aluminium trichloride in benzene
4 h;
参考文献
Matsumoto, Yonetatsu; Hayashi, Tamio; Ito, Yoshihiko
Tetrahedron, 1991 , vol. 50, # 2 p. 335 - 346
反应条件
hydrogenchloride
Ambient temperature;
参考文献
Hengge,E. et al.
Monatshefte fuer Chemie, 1975 , vol. 106, p. 887 - 892
反应条件
hydrogenchloride; aluminium trichloride in chloroform
参考文献
Ishikawa,M. et al.
Journal of Organometallic Chemistry, 1976 , vol. 118, p. 139 - 153
反应条件
1: HBr / -196 -> 45 deg C
2: LiAlH4 / diethyl ether / 0 °C
View Scheme
参考文献
Ishikawa,M. et al.
Journal of Organometallic Chemistry, 1976 , vol. 118, p. 139 - 153
反应条件
chloroform in perdeuterocyclohexane
Irradiationother disilane; var. solvents; also without CHCl3; Product distribution;
参考文献
Leigh, William J.; Sluggett, Gregory W.
Journal of the American Chemical Society, 1993 , vol. 115, # 16 p. 7531 - 7532
