2-羟基-5-甲基苯乙酮合成路线 （共 181 条）
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Ono; Imoto
Bulletin of the Chemical Society of Japan, 1936 , vol. 11, p. 127,131
Nippon Kagaku Kaishi, 1936 , vol. 57, p. 112,118
参考文献
Ono; Imoto
Bulletin of the Chemical Society of Japan, 1936 , vol. 11, p. 127,131
Nippon Kagaku Kaishi, 1936 , vol. 57, p. 112,118
反应条件
2: Pd-C(10percent) / acetic acid View Scheme
参考文献
Dinge, A. S.; Kirtany, J. K.; Paknikar, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 3 p. 245 - 246
反应条件
1: sodium hydroxide / ethanol; water / 3 h / Cooling 2: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 4 h / Reflux View Scheme
参考文献
Basawaraj, Raga; Hassappa, Ravi; Chillargi, Neelavathi; Noola, Shivanand
Indian Journal of Heterocyclic Chemistry, 2010 , vol. 19, # 3 p. 253 - 256
反应条件
1: sodium acetate 2: acetic acid; chlorine 3: H2O View Scheme
参考文献
Pendse; Limaye
Rasayanam, 1955 , vol. 2, p. 74,78
反应条件
1: 1-(2-hydroxy-5-methylphenyl)ethanone With sodium methylate in anhydrous xylene T=60°C; 2 h; Inert atmosphere; 2: 2-triphenyl(α-carboxymethylene)phosphorane imidazolide in anhydrous xylene Intramolecular Wittig reaction; 48 h; RefluxInert atmosphere;
参考文献
Upadhyay, Puspesh K.; Kumar, Pradeep
Tetrahedron Letters, 2009 , vol. 50, # 2 p. 236 - 238
反应条件
barium dihydroxide in dimethyl sulfoxide 0.00694444 h; microwave irradiation;
参考文献
Lamba; Kumar, Suresh; Makrandi
Journal of Chemical Research, 2006 , # 2 p. 133 - 134
反应条件
1: pyridine 2: 85percent KOH / pyridine / Heating View Scheme
参考文献
Thool; Ghiya
Journal of the Indian Chemical Society, 1988 , vol. 65, # 7 p. 522 - 524
反应条件
potassium carbonate; toluene-4-sulfonic acid; tetra(n-butyl)ammonium hydrogensulfate 1.) benzene, 80 deg C, 3 h, 2.) benzene, reflux, 45 min; Yield given. Multistep reaction;
参考文献
Li, Gui-Rong; Lau, Chu-Pak; Qin, Guo-Wei; Wang, Hong-Bing
Patent: US2008/214493 A1, 2008 ;
Location in patent: Page/Page column 11 ;
反应条件
1: pyridine 2: 85percent KOH / pyridine / Heating 3: sulfuric acid, glacial acetic acid View Scheme
参考文献
Adam, Waldemar; Golsch, Dieter; Hadjiarapoglou, Lazaros
Journal of Organic Chemistry, 1991 , vol. 56, # 26 p. 7292 - 7297
