2-羟基-5-氯苯乙酮合成路线 (共 106 条)
反应条件
potassium carbonate in hexane T=25°C; 12 h; Irradiation;
参考文献
Garcia, Hermenegildo; Primo, Jaime; Miranda, Miguel Angel
Synthesis, 1985 , # 9 p. 901 - 902
参考文献
Humne, Vivek; Lokahnde, Pradeep
Synthetic Communications, 2014 , vol. 44, # 7 p. 929 - 935
反应条件
1: in acetonitrile T=80°C; 0.166667 h; 2: With N-chloro-succinimide in acetonitrile T=80°C; 8 h; regioselective reaction;
参考文献
Singh, Parvinder Pal; Thatikonda, Thanusha; Kumar, K. A. Aravinda; Sawant, Sanghapal D.; Singh, Baldev; Sharma, Amit Kumar; Sharma; Singh, Deepika; Vishwakarma, Ram A.
Journal of Organic Chemistry, 2012 , vol. 77, # 13 p. 5823 - 5828
反应条件
aluminium trichloride T=180°C; 0.5 h;
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Synthetic Communications, 1996 , vol. 26, # 1 p. 67 - 74
反应条件
hydrogenchloride in ethanol; water 12 h; Heating;
参考文献
Boulton, A. J.; Tsoungas, Petros G.; Tsiamis, Chris
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 695 - 698
反应条件
sodium perborate in acetic acid deoximation; 3.5 h; Heating;
参考文献
Jadhav, Vidyadhar K.; Deshmukh, Anjali P.; Wadagaonkar, Prakash P.; Salunkhe, Manikrao M.
Synthetic Communications, 2000 , vol. 30, # 8 p. 1521 - 1527
反应条件
1: Heating 2: AlCl3 / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 5 p. 1366 - 1370
反应条件
boron tribromide in dichloromethane T=-78 - 23°C; 1 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 619 - 622
反应条件
2,2,6,6-tetramethyl-piperidine; sulfuryl dichloride T=100°C; 0.75 h; Inert atmosphere; regioselective reaction;
参考文献
Saper, Noam I.; Snider, Barry B.
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 809 - 813