2-羟基-5-氯苯乙酮合成路线 （共 106 条）
反应条件
1: potassium hydroxide / ethanol / 20 °C 2: iodine / dimethyl sulfoxide / 140 °C View Scheme
参考文献
Ghotekar; Mandhane; Joshi; Bhagat; Gill
Indian Journal of Heterocyclic Chemistry, 2010 , vol. 19, # 4 p. 341 - 344
反应条件
1: trichlorophosphate; pyridine / 0 °C / |Sonication 2: potassium hydroxide; pyridine / |Sonication 3: acetic acid / 0.27 h / 65 °C / |Sonication View Scheme
参考文献
Chate, Asha V.; Ghotekar, Dattatraya S.; Bhagat, Sunil S.; Gill, Charansingh H.
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 1 p. 149 - 154
反应条件
2: KMnO4 View Scheme
参考文献
Horton,W.J.; Robertson,D.E.
Journal of Organic Chemistry, 1960 , vol. 25, p. 1016 - 1020
反应条件
1: 87 percent / LiH / tetrahydrofuran / 3 h / Heating 2: 97 percent / AcOH; HCl / 0.05 h / Heating View Scheme
参考文献
Sosnovskikh; Usachev
Russian Chemical Bulletin, 2001 , vol. 50, # 3 p. 453 - 455
反应条件
1: 80 percent / NaOH / ethanol / 3 h / 0 °C 2: 60 percent / NaOH, 30percent H2O2 / methanol; H2O / 5 h / 0 °C View Scheme
参考文献
Gupta, Satish C.; Saini, Ashok; Kumar, Devinder; Yadav, Narender S.; Chand, Kuldeep; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 2 p. 177 - 184
反应条件
potassium hydroxide in methanol Claisen-Schmidt Condensation; 0.0333333 h; Microwave irradiation;
参考文献
Albogami, Abdullah Saad; Karama, Usama; Mousa, Ahmed Amine; Khan; Al-Mazroa, Sara Abdullah; Alkhathlan, Hamad Z.
Oriental Journal of Chemistry, 2012 , vol. 28, # 2 p. 619 - 626
反应条件
1.1: Ba(OH)2 / ethanol / 0.33 h / Reflux 1.2: Cooling with ice 2.1: benzene / 8 h / Irradiation View Scheme
参考文献
Kamboj, Ramesh C.; Berar, Surinder; Berar, Urmila; Gupta, Satish C.
Journal of the Indian Chemical Society, 2011 , vol. 88, # 6 p. 879 - 885
反应条件
1: 2 h / 80 - 90 °C 2: 70 percent / NH2OH*HCl / ethanol / 0.5 h / Heating View Scheme
参考文献
Ghosh, Tarun; Saha, Satyajit; Bandyopadhyay, Chandrakanta
Synthesis, 2005 , # 11 art. no. T14704SS, p. 1845 - 1849
反应条件
nitric acid in acetic acid 2.5 h; Ambient temperature;
参考文献
Burdeska, K.
Synthesis, 1982 , # 11 p. 940 - 942
反应条件
pyH(+)CO3(-) in acetic acid
参考文献
Patwari, Shivaji B.; Baseer, Mohammad A.; Vibhute, Yashwant B.; Bhusare, Sudhakar R.
Tetrahedron Letters, 2003 , vol. 44, # 26 p. 4893 - 4894
