2'-羟基-5'-硝基苯乙酮合成路线 （共 49 条）
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-ethane T=50°C; 2 h;
参考文献
DAEWOONG PHARMACEUTICAL CO., LTD.
Patent: WO2006/109933 A1, 2006 ;
Location in patent: Page/Page column 48 ;
反应条件
K 10 montmorillonite Fries rearrangement; 0.0666667 h; microwave irradiation;
参考文献
Kad; Trehan; Kaur; Nayyar; Arora; Brar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 7 p. 734 - 736
反应条件
nitric acid; acetic acid 1.) RT, 40 min, 2.) from 45 to 50 deg C, 16 h;
参考文献
Cushman, Mark; Zhu, Helen; Geahlen, Robert L.; Kraker, Alan J.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 20 p. 3353 - 3362
反应条件
AlCl3, aluminium chloride in dichloromethane T=-5 - 25°C;
参考文献
Du, Zhen-Ting; Lu, Jing; Yu, Hong-Rui; Xu, Yan; Li, An-Pai
Journal of Chemical Research, 2010 , # 4 p. 222 - 227
反应条件
iron nitrate (III); 1,3-di-n-butyl-imidazolium tetrafluoroborate T=60°C; 2 h;
参考文献
Rajagopal; Srinivasan
Synthetic Communications, 2003 , vol. 33, # 6 p. 961 - 966
反应条件
ytterbium(III) triflate in carbon disulfide Friedel-Crafts reaction; 6 h; Heating;
参考文献
Su, Weike; Jin, Can
Synthetic Communications, 2004 , vol. 34, # 22 p. 4199 - 4205
反应条件
potassium tert-butylate in acetonitrile T=-10°C;
参考文献
Journal of Organic Chemistry, , vol. 69, # 4 p. 1298 - 1308
反应条件
nitric acid; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 76, p. 4993
参考文献
US6214882 B1, ;
US 6214882 B1
反应条件
1: pyridine / dichloromethane 2: AlCl3, aluminium chloride / 120 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 10 p. 2855 - 2859
