2'-羟基-5'-硝基苯乙酮合成路线 （共 49 条）
反应条件
hydroxylamine hydrochloride; sodium hydroxide in ethanol; water
参考文献
Kociolek, Martin G.; Hoermann, Olivia
Synthetic Communications, 2012 , vol. 42, # 17 p. 2632 - 2638
反应条件
1: 84.3 percent / K2CO3 / acetone / 3 h / Heating
2: 90 percent / K2CO3 / H2O / 0.67 h / Heating
3: 34.2 percent / AcONa, Ac2O / 3 h / 110 °C
View Scheme
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
反应条件
1: 84.3 percent / K2CO3 / acetone / 3 h / Heating
2: 90 percent / K2CO3 / H2O / 0.67 h / Heating
View Scheme
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
反应条件
1: 84.3 percent / K2CO3 / acetone / 3 h / Heating
2: 90 percent / K2CO3 / H2O / 0.67 h / Heating
3: 56.9 percent / AcONa, Ac2O / 3 h / 110 °C
View Scheme
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
反应条件
potassium carbonate in acetone
3 h; Heating;
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
反应条件
potassium carbonate in acetone
T=20°C;
参考文献
Zhong, Zhenlin; Snowden, Timothy S.; Best, Michael D.; Anslyn, Eric V.
Journal of the American Chemical Society, 2004 , vol. 126, # 11 p. 3488 - 3495
参考文献
Asahi Kasei Kogyo Kabushiki Kaisha
Patent: US6037362 A1, 2000 ;
反应条件
potassium carbonate; acetone
参考文献
Thanawalla et al.
Journal of the Indian Chemical Society, 1959 , vol. 36, p. 674
反应条件
1: ammonia / methanol / 2 h / 20 °C / Inert atmosphere
2: N-chloro-succinimide; potassium carbonate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Chen, Cheng-Yi; Andreani, Teresa; Li, Hongmei
Organic Letters, 2011 , vol. 13, # 23 p. 6300 - 6303
