(2-丁烯-1-基氧基)苯合成路线 (共 13 条)
反应条件
1: With C6H10BBr3 in dichloromethane T=20°C; 0.0833333 h; Inert atmosphere; 2: Claisen rearrangement;
参考文献
Yao, Min-Liang; Reddy, Marepally Srinivasa; Zeng, Wenbin; Hall, Kelly; Walflsh, Ingrid; Kabalka, George W.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1385 - 1387
反应条件
10 Pd on charcoal; diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in ethanol 4 h; Reflux;
参考文献
Liu, Qiang; Li, Jing; Shen, Xiao-Xia; Xing, Rui-Guang; Yang, Jie; Liu, Zhengang; Zhou, Bo
Tetrahedron Letters, 2009 , vol. 50, # 9 p. 1026 - 1028
反应条件
triphenylphosphine; Bu4N[Fe(CO)3(NO)] in tert-butyl methyl ether
T=80°C; regioselective reaction;
参考文献
Trivedi, Rushi; Tunge, Jon A.
Organic Letters, 2009 , vol. 11, # 24 p. 5650 - 5652
反应条件
potassium carbonate; acetone
参考文献
Claisen; Tietze
Chemische Berichte, 1926 , vol. 59, p. 2349
Full Text Show Details
v. Braun; Schirmacher
Chemische Berichte, 1923 , vol. 56, p. 544
反应条件
palladium(II) 2,4-pentanedionate
T=80°C; 1 h; Schlenk techniqueInert atmosphereHigh pressure;
参考文献
Hausoul, Peter J. C.; Eggenhuisen, Tamara M.; Nand, Deepak; Baldus, Marc; Weckhuysen, Bert M.; Klein Gebbink, Robertus J. M.; Bruijnincx, Pieter C. A.
Catalysis Science and Technology, 2013 , vol. 3, # 10 p. 2571 - 2579
反应条件
2: potassium carbonate; acetone
View Scheme
参考文献
Claisen; Tietze
Chemische Berichte, 1926 , vol. 59, p. 2349
参考文献
Claisen; Tietze
Chemische Berichte, 1926 , vol. 59, p. 2349
参考文献
Claisen; Tietze
Chemische Berichte, 1926 , vol. 59, p. 2349
Full Text Show Details
v. Braun; Schirmacher
Chemische Berichte, 1923 , vol. 56, p. 544
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether
T=20°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.; Lomakina, S. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 1939 - 1945
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 9 p. 2159 - 2166
反应条件
(i) B2H6, (ii) aq. H2O2, aq. NaOH; Multistep reaction;
参考文献
Brown,H.C.; Gallivan,R.M.
Journal of the American Chemical Society, 1968 , vol. 90, # 11 p. 2906 - 2915