1-(4-氯苯基)-3-丁烯-1-醇合成路线 (共 47 条)
反应条件
antimony in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide 15 h; Heating;
参考文献
Butsugan, Yasuo; Ito, Hirokazu; Araki, Shuki
Tetrahedron Letters, 1987 , vol. 28, # 32 p. 3707 - 3708
反应条件
N-chloro-succinimide; tin(ll) chloride in dichloromethane T=-60°C; 33 h;
参考文献
Masuyama; Saeki; Horiguchi; Kurusu
Synlett, 2001 , # 11 p. 1802 - 1804
反应条件
tin(IV) chloride; tetra-(n-butyl)ammonium iodide in dichloromethane T=20°C; 24 h;
参考文献
Masuyama, Yoshiro; Suga, Takanori; Watabe, Akiko; Kurusu, Yasuhiko
Tetrahedron Letters, 2003 , vol. 44, # 14 p. 2845 - 2847
反应条件
water; ammonium chloride; β-cyclodextrin; zinc T=60°C; 8 h;
参考文献
Reddy, M. Somi; Narender; Nageswar; Rao, K. Rama
Synthetic Communications, 2007 , vol. 37, # 12 p. 1983 - 1988
反应条件
bis-triphenylphosphine-palladium(II) chloride; tin(ll) chloride in water T=49.84°C; Barbier reaction; 12 h;
参考文献
Huang, Jianlin; Zhang, Fang
Applied Organometallic Chemistry, 2010 , vol. 24, # 11 p. 767 - 773
反应条件
benzene-1,2-diol; triethylamine in chloroform Heating;
参考文献
Hosomi, Akira; Kohra, Shinya; Ogata, Koichiro; Yanagi, Toshiharu; Tominaga, Yoshinori
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2415 - 2420
反应条件
in diethyl ether T=-78 - 0°C; 1.5 h;
参考文献
Shen, Kao-Hsien; Yao, Ching-Fa
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3980 - 3983
反应条件
in dichloromethane; water T=20°C; 4 h;
参考文献
Arnauld, Thomas; Barrett, Anthony G.M; Seifried, Robert
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7899 - 7901
反应条件
silver(I) acetate in toluene T=100°C; 15 h;
参考文献
Itami, Kenichiro; Kamei, Toshiyuki; Mineno, Masahiro; Yoshida, Jun-Ichi
Chemistry Letters, 2002 , # 11 p. 1084 - 1085
反应条件
diethylzinc in hexane; dichloromethane Ambient temperature;
参考文献
Huang, Wen-Hua; Huang, Yao-Zeng; Dai, Li-Xin
Tetrahedron Letters, 1998 , vol. 39, # 38 p. 6953 - 6956