反应条件
1: 83 percent / thionyl chloride / toluene / 12 h / 25 °C 2: 90 percent / 1.) n-BuLi, / diethyl ether / 1.) -78 deg C, 15 min, 0 deg C, 30 min 3: 92 percent / 1.) t-Bu4N(+)HSO4(-), 3M sodium hypochlorite, 2.) 5percent aq. KOH / 1.) ethyl acetate, water, 20 deg C, 12 h, 2.) water, MeOH, 20 deg C, 12 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 173 - 182
