4-(1-苄基-吡咯烷-3-基)吡啶合成路线 （共 4 条）
反应条件
1: 91 percent / ammonium formate / Pd/C / methanol / 8 h / 80 - 90 °C 2: triethylamine / tetrahydrofuran / 30 °C View Scheme
参考文献
Kurkin; Sumtsova; Yurovskaya
Chemistry of Heterocyclic Compounds, 2007 , vol. 43, # 1 p. 34 - 40
反应条件
ammonium formate; palladium on activated charcoal in methanol T=80 - 90°C; 8 h;
参考文献
Kurkin; Sumtsova; Yurovskaya
Chemistry of Heterocyclic Compounds, 2007 , vol. 43, # 1 p. 34 - 40
反应条件
1: in dichloromethane
T=-5°C; 0.5 h;
2: With trifluoroacetic acid in dichloromethane
6 h;
参考文献
Kurkin; Sumtsova; Yurovskaya
Chemistry of Heterocyclic Compounds, 2007 , vol. 43, # 1 p. 34 - 40
反应条件
1.1: acetonitrile / 12 h / 90 - 100 °C
2.1: H2O / 4 h / 0 - 15 °C
3.1: CH2Cl2 / 0.5 h / -5 °C
3.2: 82 percent / trifluoroacetic acid / CH2Cl2 / 6 h
View Scheme
参考文献
Kurkin; Sumtsova; Yurovskaya
Chemistry of Heterocyclic Compounds, 2007 , vol. 43, # 1 p. 34 - 40
