反应条件
1: sodium hydrogencarbonate; potassium iodide / N,N-dimethyl acetamide / 28 h / 75 °C 2: ammonium chloride / N,N-dimethyl acetamide / 7 h / 100 °C 3: 5 palladium on charcoal; hydrogen / methanol / 2 h / 15 - 30 °C / 1125.11 Torr 4: ammonia / methanol / 20 h / 20 °C View Scheme
参考文献
ERREGIERRE S.p.A.; Ferrari, Massimo; De Zani, Daniele; Bonaldi, Matteo
Patent: EP2647625 A1, 2013 ;
