反应条件
in tetrahydrofuran absence of air and moisture; bubbling MeSH through NaH suspn. (0°C, 2 min), addn. of excess MeNCS, addn. of Mn-complex, warming to room temp. during 2 h; evapn., extn. into CH2Cl2, evapn., chromy. (SiO2, hexane, then CH2Cl2/hexane=1:9, 1:4, 1:2); IR spectroscopy;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1247 - 1255