in further solvent(s) addn. of I2 to a soln. of 1 g RuF5 in 5 ml IF5 under exclusion of moisture; heating;; distn. remained RuF5 in high vac.;;
参考文献
Holloway, J. H.; Peacock, R. D.
Journal of the Chemical Society, 1963 , p. 3892 - 3893
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Gmelin Handbook: Ru: SVol., 78, page 262 - 264
dichloromethane in dichloromethane byproducts: CHCl2F, HF, CH2ClF; inert atmosphere; excess of CH2Cl2, warming to room temp.; further byproducts;
参考文献
Dukat, Wolfgang W.; Holloway, John H.; Hope, Eric G.; Rieland, Matthias R.; Townson, Paul J.; Powell, Richard L.
Journal of the Chemical Society, Chemical Communications, 1993 , # 18 p. 1429 - 1430
H2 in neat (no solvent)
react. with H2 in a Ni bomb at 230 °C for 4 h; formation of a solid black product of Ru with absorbed HF;;
参考文献
Gmelin Handbook: Ru: SVol., 79, page 264 - 266
Full Text Show Details
Farrar, R. L.; Barber, E. J.; Capps, R. H.; Skidmore, M. R.; Bernhardt, H. A.
N. S. A., AECD-3468 (1950/52), S. 1/20 1953 , vol. 7, p. 529
