2,4-二氟-2-羟基苯乙酮合成路线 (共 3 条)
反应条件
hydrogenchloride in methanol T=40°C; 5 h;
参考文献
Miyauchi, Hiroshi; Nakamura, Toshio; Ohashi, Naohito
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 9 p. 2625 - 2632
反应条件
potassium phosphate buffer; thiamine diphosphate; magnesium sulfate; benzaldehyde lyase from Pseudomonas fluorescens in dimethyl sulfoxide T=37°C; pH=7.0; Enzymatic reaction;
参考文献
Demir, Ayhan S.; Ayhan, Peruze; Igdir, A. Cigdem; Duygu, A. Nese
Tetrahedron, 2004 , vol. 60, # 31 p. 6509 - 6512
反应条件
1: 94 percent / dimethylformamide / 4 h / Ambient temperature 2: 69 percent / 1 M aq. HCl / methanol / 5 h / 40 °C View Scheme
参考文献
Miyauchi, Hiroshi; Nakamura, Toshio; Ohashi, Naohito
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 9 p. 2625 - 2632