3-氨基-4-乙酰氨基吡啶合成路线 （共 8 条）
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; Hydrogenation; P=5250.42 Torr; 23 h;
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
1: 97 percent / Et3N / acetonitrile / 1 h / 20 °C 2: 72 percent / N2O5 / nitromethane / 0.17 h / 0 °C 3: 97 percent / H2 / 5 percent Pd/C / methanol / 23 h / 20 °C / 5250.42 Torr View Scheme
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
1: 72 percent / N2O5 / nitromethane / 0.17 h / 0 °C 2: 97 percent / H2 / 5 percent Pd/C / methanol / 23 h / 20 °C / 5250.42 Torr View Scheme
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
1: N-(3-aminopyridin-4-yl)acetamide With NOBF4 in acetonitrile T=0°C; 0.333333 h; 2: benzylamine in acetonitrile T=20°C;
参考文献
Holt, Jarle; Fiksdahl, Anne
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 2 p. 417 - 423
反应条件
1: N-(3-aminopyridin-4-yl)acetamide With NOBF4 in acetonitrile T=0°C; 0.333333 h; 2: isopropylamine in acetonitrile T=20°C;
参考文献
Holt, Jarle; Fiksdahl, Anne
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 2 p. 417 - 423
反应条件
1: N-(3-aminopyridin-4-yl)acetamide With NOBF4 in acetonitrile T=0°C; 0.333333 h; 2: benzylamine in acetonitrile T=20°C;
参考文献
Holt, Jarle; Fiksdahl, Anne
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 2 p. 417 - 423
反应条件
acetic acid Cyclization; 1.5 h; Heating;
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
1: N-(3-aminopyridin-4-yl)acetamide With NOBF4 in acetonitrile
T=0°C; 0.333333 h;
2: isopropylamine in acetonitrile
T=20°C;
参考文献
Holt, Jarle; Fiksdahl, Anne
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 2 p. 417 - 423
