反应条件
1: triethylamine; diphenyl phosphoryl azide / 1,2-dichloro-ethane / 5 h / 20 °C / |Inert atmosphere; |Reflux 2: titanium(IV) isopropylate / toluene / 12 h / 80 °C / |Inert atmosphere 3: hydrogenchloride / water; 1,4-dioxane / 24 h / |Reflux 4: sodium hydrogencarbonate / water; 1,4-dioxane / 0.33 h / 0 °C View Scheme
参考文献
Banerjee, Souvik; Wiggins, Walker J.; Geoghegan, Jessie L.; Anthony, Catherine T.; Woltering, Eugene A.; Masterson, Douglas S.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 37 p. 6307 - 6319
