1,8-萘啶-2,7-二胺合成路线 （共 9 条）
反应条件
ammonia in ethanol T=180°C; 24 h;
参考文献
Corbin; Zimmerman; Thiessen; Hawryluk; Murray
Journal of the American Chemical Society, 2001 , vol. 123, # 43 p. 10475 - 10488
反应条件
ammonium hydroxide T=180°C; 24 h;
参考文献
Corbin; Zimmerman; Thiessen; Hawryluk; Murray
Journal of the American Chemical Society, 2001 , vol. 123, # 43 p. 10475 - 10488
反应条件
sodium amide in xylene T=130°C; 12 h;
参考文献
Goswami, Shyamaprosad; Mukherjee, Reshmi; Mukherjee, Rakhi; Jana, Subrata; Maity, Annada C.; Adak, Avijit Kumar
Molecules, 2005 , vol. 10, # 8 p. 929 - 936
反应条件
1: 60 percent / POCl3 / 1.5 h / 90 - 95 °C 2: 83 percent / pyridine / 48 h / Heating 3: 95 percent / aq. HCl / 2 h / Heating View Scheme
参考文献
Corbin; Zimmerman; Thiessen; Hawryluk; Murray
Journal of the American Chemical Society, 2001 , vol. 123, # 43 p. 10475 - 10488
反应条件
1: 85 percent / 2.5 h / Heating 2: 60 percent / POCl3 / 1.5 h / 90 - 95 °C 3: 74 percent / NH3 / ethanol / 24 h / 180 °C View Scheme
参考文献
Dey, Swapan; Sain, Dibyendu; Goswami, Shyamaprosad
RSC Advances, 2014 , vol. 4, # 1 p. 428 - 433
反应条件
hydrogenchloride 2 h; Heating;
参考文献
Park, Taiho; Mayer, Michael F.; Nakashima, Shoji; Zimmerman, Steven C.
Synlett, 2005 , # 9 art. no. S02405ST, p. 1435 - 1436
反应条件
acetic acid; zinc 3 h; Heating;
参考文献
Goswami, Shyamaprosad; Mukherjee, Reshmi; Mukherjee, Rakhi; Jana, Subrata; Maity, Annada C.; Adak, Avijit Kumar
Molecules, 2005 , vol. 10, # 8 p. 929 - 936
反应条件
copper(I) oxide; ammonium hydroxide; water in ethylene glycol T=90°C; 12 h; Inert atmosphere;
参考文献
Anderson, Cyrus A.; Taylor, Phillip G.; Zeller, Mary A.; Zimmerman, Steven C.
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4848 - 4851
反应条件
1.1: sulfuric acid / 3 h / 80 - 90 °C 2.1: trichlorophosphate / 1 h / |Reflux 2.2: 4 h / |Reflux 2.3: 3 h / |Reflux View Scheme
参考文献
Dey, Swapan; Sain, Dibyendu; Goswami, Shyamaprosad
RSC Advances, 2014 , vol. 4, # 1 p. 428 - 433
